ꢀꢀꢀꢁ
920ꢀ ꢀK. Kraushaar et al.: Insertion of phenyl isocyanate into mono- and diaminosilanes
4.2.4 Boiling and melting points
within the research group “Chemical utilization of carbon
dioxide with aminosilanes (CO2Sil)” that is financially
We have developed a fast method to determine the boiling supported by the European Union (European regional
point of small samples under inert atmosphere using development fund), the Ministry of Science and Art of
standard Schlenk technique. A measurement only takes Saxony (SMWK) and the Sächsische Aufbaubank (SAB).
about 15 min and the sample volume should be 0.05–
0.2 mL. Boiling points up to 300°C can be measured with
our low cost glassware apparatus by recording the tem-
References
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5 Supporting Information
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Acknowledgements: The authors thank Freistaat Sachsen
for financial support. Part of this work was performed
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