Bioorganic and Medicinal Chemistry p. 419 - 421 (1996)
Update date:2022-08-03
Topics:
Baeckstroem, Peter
Koutek, Bohumir
Saman, David
Vrkoc, Jan
trans-Sabinene hydrate (1), was synthesized from (-)-3-thujol (2) in four steps. The key step was the selective formation of trans-2-hydroxy-3-thujene (6) by photooxygenation of a 3:1 mixture of 2- and 3-thujenes (4 and 5) obtained from (-)-3-thujol mesylate (3). Hydrogenation of 6 gave compound 1 in 46% overall yield.
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