Synthetic Communications p. 313 - 324 (2000)
Update date:2022-08-11
Topics:
Hallouis, Sophie
Saluzzo, Christine
Amouroux, Roger
The one step transformation of esters into secondary alcohols (70-80% yields) has been performed with a Grignard reagent in the presence of calcium or zinc borohydride. Under the same conditions, vinylic Grignard reagents gave γ,δ-unsaturated alcohols in good yields through three successive reactions: addition to the ester carbonyl, then conjugate addition and, finally reduction).
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