Tetrahedron Letters p. 5435 - 5436 (1996)
Update date:2022-08-10
Topics:
Bailey, William F.
Punzalan, Eric R.
2-(2-Propenoxy)phenyllithium (1), which may be prepared from the corresponding iodide by low-temperature lithium-iodine exchange, rearranges on warming in the presence of TMEDA via 5-exo cyclization to (2,3-dihydrobenzofuranyl)methyllithium (2) followed by γ-elimination to give variable amounts of the lithium salt of 2-(cyclopropyl)phenol (3).
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