Tetrahedron Letters p. 799 - 802 (2018)
Update date:2022-08-29
Topics:
Shi, Jianjun
Niwayama, Satomi
The highly efficient selective monohydrolysis reaction we previously reported has been applied to monohydrolysis of several bulkyl symmetric diesters, including diethyl esters, dipropyl esters, and dibutyl esters. A greater proportion of a polar aprotic co-solvent, DMSO, and aqueous KOH appear to help improve the reactivity of bulky diesters compared to the corresponding dimethyl esters. The procedure is mild and practical, yielding the corresponding half-esters in high yields under simple conditions.
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Doi:10.1016/j.bmcl.2016.07.007
(2016)Doi:10.1246/cl.1979.713
(1979)Doi:10.1016/j.ejmech.2017.12.088
(2018)Doi:10.1021/op8000178
(2008)Doi:10.1007/BF02253231
(1997)Doi:10.1055/s-0032-1316819
(2013)