Organic Process Research and Development p. 1759 - 1762 (2014)
Update date:2022-08-11
Topics:
Tortoioli, Simone
Marchal, Daniel
Kesselgruber, Martin
Pabst, Thomas
Skranc, Wolfgang
Abele, Stefan
A three-step fully telescoped synthesis of an N-sulfonyl proline amide, a nonpeptide antagonist of human orexin receptors, is described. The process development from the medicinal chemistry route up to the 240 kg production of 1 is discussed with a focus
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Doi:10.1002/anie.201607940
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