Bulletin of the Chemical Society of Japan p. 2313 - 2318 (1995)
Update date:2022-08-28
Topics:
Okuma, Kentaro
Ikari, Komei
Ono, Masaaki
Sato, Yasunari
Kuge, Seiji
et al.
Reactions of (dimethylamino)phenylsulfoxonium mathylide with triphenylvinylphosphonium salts gave the corresponding cyclopropyltriphenylphosphonium salts (E-form) in high yields, when 1,8-diazabicyclo<5.4.0>undec-7-ene was used as a base.Reactions of cyclopropyltriphenylphosphonium salts with sodium hydride in the presence of tris<2-(2-methoxyethoxy)ethyl>amine afforded the corresponding ylides, which further reacted with aldehydes to give alkylidenepropanes in high yields.
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