Synthetic Communications p. 3085 - 3088 (2011)
Update date:2022-08-16
Topics:
Shi, Enxue
Xiao, Junhua
Pei, Chengxin
Chen, Jisheng
A rapid, efficient, solvent-free, and catalyst-free procedure has been developed for the synthesis of pseudohalophosphates from phosphorochloridate and sodium (or potassium) pseudohalides under microwave irradiation. Diethyl, diisobutyl, and diphenyl phosphorazidates, phosphorocyanidates, and phosphor(isothiocyanidate)s 2a-2i were prepared in good yields under mild conditions. Copyright
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Doi:10.1021/jacs.6b00882
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