Russian Chemical Bulletin p. 1157 - 1161 (1996)
Update date:2022-08-28
Topics:
Fedorov
Golovina
Arakcheeva
Trofimova
Atovmyan
A novel reaction of the sodium salt of 2-nitroethanol in aqueous ammonia resulted in the sodium salt of 2-oxo-3-hydroxypropionic acid oxime (1) has been found. Bromination of 1 affords 2-bromo-2-nitropropane-1,3-diol (2) with a previously unknown molecular conformation. The formation mechanisms of compounds 1 and 2 were suggested. X-ray analysis of products 1, 2 and that of the model compound, 2,2-dinitropropane-1,3-diol, was performed.
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