Journal of Organic Chemistry p. 361 - 364 (1994)
Update date:2022-08-25
Topics:
Vasudevan
Watt
A selective hydrolysis of 1,4,6-trioxaspiro[4.5]decane orthoesters by 2,3- dichloro-5,6-dicyanoquinone (DDQ) in aqueous acetone in the presence of other acid-sensitive ketals is suggested to involve the formation of a charge- transfer complex followed by hydrolysis. A hydride-transfer mechanism for this oxidation was excluded.
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