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Cas Database

Name	Phenyl bromoacetate	EINECS	805-881-2
CAS No.	620-72-4	Density	1.533 g/cm³
PSA	26.30000	LogP	1.98690
Solubility	Soluble in ethanol and ether, insoluble in water.	Melting Point	31-33 °C(lit.)
Formula	C₈H₇BrO₂	Boiling Point	261.9 °C at 760 mmHg
Molecular Weight	215.046	Flash Point	112.2 °C
Transport Information	N/A	Appearance	Liquid
Safety	24/25	Risk Codes	N/A
Molecular Structure		Hazard Symbols	N/A
Synonyms	Aceticacid, bromo-, phenyl ester (6CI,7CI,8CI,9CI);alpha-Phenyl Bromoacetate;Phenyl a-bromoacetate;bromoacetic acidphenyl ester;	Article Data	32

Phenyl bromoacetate Synthetic route

: 598-21-0
2-Bromoacetyl bromide

: 108-95-2
phenol

: 620-72-4
phenyl 2-bromoacetate

Conditions

Conditions	Yield
Heating;	92%
With triethylamine In dichloromethane at 0℃; for 1.5h; Inert atmosphere;	81%
at 80℃; for 1h;	77%

: 100-66-3
methoxybenzene

: 598-21-0
2-Bromoacetyl bromide

: 620-72-4
phenyl 2-bromoacetate

Conditions

Conditions	Yield
With zinc(II) chloride at 50 - 70℃; for 3.5h;	38%

: 79-08-3
bromoacetic acid

: 108-95-2
phenol

: 620-72-4
phenyl 2-bromoacetate

Conditions

Conditions	Yield
(i) DCC, THF, (ii) /BRN= 506167/; Multistep reaction;
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃;

<β.β-dibromo-vinyl>-phenyl ether: <β.β-dibromo-vinyl>-phenyl ether

: 620-72-4
phenyl 2-bromoacetate

Conditions

Conditions	Yield
With acetic acid at 100℃; im geschlossenen Rohr;

bromoacetimidic acid phenyl ester hydrochloride: bromoacetimidic acid phenyl ester hydrochloride

: 620-72-4
phenyl 2-bromoacetate

Conditions

Conditions	Yield
With water

: 7647-01-0
hydrogenchloride

: 60-29-7
diethyl ether

: bromoethynyl-phenyl ether

: 1600-27-7
mercury(II) diacetate

: 620-72-4
phenyl 2-bromoacetate

Conditions

Conditions	Yield
at 10℃;

: 7732-18-5
water

: 2-bromo-acetimidic acid phenyl ester; hydrochloride

: 620-72-4
phenyl 2-bromoacetate

: 106-41-2
4-bromo-phenol

: 620-72-4
phenyl 2-bromoacetate

Conditions

Conditions	Yield
With sulfuric acid In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; acetic anhydride

: 620-72-4
phenyl 2-bromoacetate

: 74802-29-2
3S-3-<<(1,1-Dimethylethoxy)carbonyl>amino>-2,5-dioxo-2,3,4,5-tetrahydro-1H-1-benzazepine

: 128776-36-3
Benzyl 2-(3S-3-<<(1,1-Dimethylethoxy)carbonyl>amino>-2,5-dioxo-2,3,4,5-tetrahydro-1H-1-benzazepin-1-yl)-ethanoate

Conditions

Conditions	Yield
With tetrabutylammomium bromide; potassium carbonate In acetone	98%

: 620-72-4
phenyl 2-bromoacetate

: 603-35-0
triphenylphosphine

: 32443-55-3
((triphenyl)-λ5-phosphanylidene)acetic acid phenyl ester

Conditions

Conditions	Yield
Stage #1: phenyl 2-bromoacetate; triphenylphosphine In chloroform at 23℃; Inert atmosphere; Stage #2: With sodium hydroxide In water	96%
Stage #1: phenyl 2-bromoacetate; triphenylphosphine In benzene at 20℃; for 18h; Stage #2: With sodium hydroxide In dichloromethane; water for 0.5h;
Multi-step reaction with 2 steps 1: toluene / 12 h / Inert atmosphere 2: sodium hydroxide / dichloromethane; water / 0.33 h / 20 °C View Scheme

Phenyl bromoacetate Chemical Properties

Product Name: Phenyl bromoacetate (CAS NO.620-72-4)

Molecular Formula: C₈H₇BrO₂
Molecular Weight: 215.04g/mol
Mol File: 620-72-4.mol
Melting Point: 31-33 °C(lit.)
Boiling point: 261.9 °C at 760 mmHg
Flash Point: 112.2 °C
Density: 1.533 g/cm³
Surface Tension: 43.8 dyne/cm
Enthalpy of Vaporization: 49.97 kJ/mol
Vapour Pressure: 0.0112 mmHg at 25°C
Product Categories: C8 to C9; Carbonyl Compounds; Esters

Phenyl bromoacetate Specification

Phenyl bromoacetate , its CAS NO. is 620-72-4, the synonym is alpha-Phenyl Bromoacetate .

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