Benzeneacetonitrile, a-oxo-, N-oxide

Base Information

• Chemical Name: Benzeneacetonitrile, a-oxo-, N-oxide
• CAS No.: 31879-18-2
• Molecular Formula: C8H5NO2
• Molecular Weight: 147.133
• Mol file: 31879-18-2.mol

Synonyms:

Chemical Property of Benzeneacetonitrile, a-oxo-, N-oxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzeneacetonitrile, a-oxo-, N-oxide

There total 2 articles about Benzeneacetonitrile, a-oxo-, N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Phenyl-2-oxoethanehydroxamoyl chloride → phenylglyoxylonitrile oxide (31879-18-2)

Guidance literature:

With triethylamine; In diethyl ether;

DOI:10.1021/ja00393a012

Reference yield:

→ phenylglyoxylonitrile oxide (31879-18-2)

Guidance literature:

α-Chloro-α-hydroxyiminoacetophenon 8, Triethylamin;

DOI:10.1246/bcsj.51.1495

Reference yield: 90.0%

9-(1-methylethylidene)-1,4-dihydro-1,4-methanonaphthalene (7350-72-3) + phenylglyoxylonitrile oxide (31879-18-2) → C22H19NO2 (76673-21-7)

Guidance literature:

In diethyl ether; for 24h; Ambient temperature;

DOI:10.1021/ja00393a012

Downstream raw materials:

(Z)-N-hydroxy-α-oxobenzeneethanimidoyl chloride

3,4-dibenzoyl-1,2,5-oxadiazole-N-oxide

Benzoic acid (1S,2S,6R,7S)-5-benzoyl-3-oxa-4-aza-tricyclo[5.2.1.0^2,6]deca-4,8-dien-10-yl ester

Benzoic acid (1R,2S,6R,7R)-5-benzoyl-3-oxa-4-aza-tricyclo[5.2.1.0^2,6]deca-4,8-dien-10-yl ester