Technology Process of Benzenediazonium, 2-benzoyl-, tetrafluoroborate(1-)
There total 4 articles about Benzenediazonium, 2-benzoyl-, tetrafluoroborate(1-) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrafluoroboric acid; isopentyl nitrite;
In
ethanol; water;
at -5 ℃;
for 0.5h;
DOI:10.1021/jo00183a021
- Guidance literature:
-
2-acetamidobenzophenone;
With
boron trifluoride - methanol (1/1);
In
methanol;
at 80 ℃;
for 16h;
With
tert.-butylnitrite;
In
methanol;
at 0 ℃;
for 2h;
Concentration;
DOI:10.1021/acs.joc.5b00272
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: palladium diacetate; trifluoroacetic acid; sodium dodecyl sulfate; tert.-butylhydroperoxide / water / 24 h / 20 °C
2.1: boron trifluoride - methanol (1/1) / methanol / 16 h / 80 °C
2.2: 2 h / 0 °C
With
tert.-butylhydroperoxide; boron trifluoride - methanol (1/1); palladium diacetate; sodium dodecyl sulfate; trifluoroacetic acid;
In
methanol; water;
DOI:10.1021/acs.joc.5b00272
