1,2,3,4,5,6,7,8,9,10-Decahydroanthracene

Base Information

• Chemical Name: 1,2,3,4,5,6,7,8,9,10-Decahydroanthracene
• CAS No.: 3485-60-7
• Molecular Formula: C14H20
• Molecular Weight: 188.313
• DSSTox Substance ID: DTXSID80496346
• Wikidata: Q82345138
• Mol file: 3485-60-7.mol

Synonyms:1,2,3,4,5,6,7,8,9,10-DECAHYDROANTHRACENE;3485-60-7;DTXSID80496346

Chemical Property of 1,2,3,4,5,6,7,8,9,10-Decahydroanthracene

Chemical Property:

• XLogP3: 3.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 188.156500638
• Heavy Atom Count: 14
• Complexity: 244

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCC2=C(C1)CC3=C(C2)CCCC3

Technology Process of 1,2,3,4,5,6,7,8,9,10-Decahydroanthracene

There total 6 articles about 1,2,3,4,5,6,7,8,9,10-Decahydroanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

anthracene (120-12-7) → 1,2,3,4,5,6,7,8,9,10-hexahydroanthracene (3485-60-7) + 1,4,5,8,9,10-hexahydroanthracene (5910-28-1)

Guidance literature:

With white sand; calcium; tert-butyl alcohol; In tetrahydrofuran; ethylenediamine; at 0 ℃; for 24h; Yield given;

DOI:10.1016/S0040-4039(01)81168-0

Reference yield: 52.3%

anthracene (120-12-7) → 9,10-dihydroanthracene (613-31-0) + 1,2,3,4,5,6,7,8,9,10-hexahydroanthracene (3485-60-7) + 1,2,3,4-tetrahydroanthracene (2141-42-6) + 1,2,3,4,5,6,7,8-octahydroanthracene (1079-71-6)

Guidance literature:

With hydrogen; lithium aluminium tetrahydride; titanium tetrachloride; In n-heptane; at 200 ℃; for 3h; under 67505.4 Torr; Further byproducts given;

Reference yield: 28.0%

anthracene (120-12-7) → 9,10-dihydroanthracene (613-31-0) + 1,2,3,4,5,6,7,8,9,10-hexahydroanthracene (3485-60-7) + 1,2,3,4,9,10,11,12-octahydroanthracene (7389-11-9,85281-16-9) + 1,2,3,4-tetrahydroanthracene (2141-42-6) + 1,2,3,4,5,6,7,8-octahydroanthracene (1079-71-6)

Guidance literature:

With hydrogen; lithium aluminium tetrahydride; titanium tetrachloride; In n-heptane; at 200 ℃; for 3h; under 67505.4 Torr; Product distribution; other conditions: other solvents (diglyme, nonane, hexane), other times, other catalysts, other reagents (D₂O, H₂O/LiAlD₄), other temperatures;;

upstream raw materials:

anthracene

Downstream raw materials:

1,2,3,4,5,6,7,8-octahydroanthracene

Refernces

• 1、 Kariv-Miller, Essie,Pacut, Ryszard I.. "Electroreduction in Aqueous Media, Saturation of Polycyclic Aromatics.". . p. 2185 - 2192. Retrieved 2007/10/02.