Technology Process of 1,3-Dioxan-2-one, 4-phenyl-
There total 11 articles about 1,3-Dioxan-2-one, 4-phenyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetraphenyl stibonium iodide;
at 100 ℃;
for 4h;
under 36775.4 Torr;
- Guidance literature:
-
With
pyridine;
In
dichloromethane;
DOI:10.1139/v02-126
- Guidance literature:
-
carbon dioxide; 1-phenyl-1,3-propanediol;
With
1,8-diazabicyclo[5.4.0]undec-7-ene;
In
chloroform;
at 20 ℃;
for 2h;
under 760.051 Torr;
With
triethylamine; p-toluenesulfonyl chloride;
In
chloroform;
at 20 ℃;
for 16h;
DOI:10.1039/c5ra07290e