Undecanal, 10-oxo-

Base Information

• Chemical Name: Undecanal, 10-oxo-
• CAS No.: 36219-78-0
• Molecular Formula: C11H20O2
• Molecular Weight: 184.279
• Mol file: 36219-78-0.mol

Synonyms:

Chemical Property of Undecanal, 10-oxo-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Undecanal, 10-oxo-

There total 1 articles about Undecanal, 10-oxo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

undecane-1,10-diol (10596-05-1) → 10-oxo-undecanoic acid (676-00-6) + 10-oxo-undecanal (36219-78-0)

Guidance literature:

With 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; potassium bromide; In dichloromethane; at 10 - 15 ℃; for 0.166667h; pH 9.5;

DOI:10.1021/jo00273a038

Reference yield: 97.0%

10-oxo-undecanal (36219-78-0) → 1-dodecen-11-one (5009-33-6)

Guidance literature:

With boron trifluoride diethyl etherate; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1055/s-1998-36073

Reference yield: 96.0%

diiodomethane (75-11-6) + 10-oxo-undecanal (36219-78-0) → 1-dodecen-11-one (5009-33-6)

Guidance literature:

With trimethylaluminum; zinc; at 25 ℃; for 4h;

DOI:10.1016/S0040-4039(01)80893-5

upstream raw materials:

undecane-1,10-diol

Downstream raw materials:

1-dodecen-11-one

3-Hydroxy-1-phenyl-1,12-tridecanedione

13-(Dimethyl-phenyl-silanyl)-11-hydroxy-tridec-12-yn-2-one

3-Hydroxy-2-methyl-12-oxo-tridecanethioic acid S-tert-butyl ester

Refernces