Technology Process of 1,1'-(2-Ethoxyethene-1,1-diyl)dibenzene
There total 10 articles about 1,1'-(2-Ethoxyethene-1,1-diyl)dibenzene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
chloropyridinecobaloxime(III); 9-(2-mesityl)-10-methylacridinium perchlorate;
In
acetonitrile;
at 20 ℃;
for 12h;
Irradiation;
Inert atmosphere;
Schlenk technique;
DOI:10.1002/anie.201609274
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere
2: tris-(dibenzylideneacetone)dipalladium(0); triphenylphosphine; caesium carbonate / tetrahydrofuran / 4 h / Inert atmosphere; Reflux
With
tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate; triphenylphosphine;
In
tetrahydrofuran;
1: |Miyaura Borylation Reaction / 2: |Suzuki-Miyaura Coupling;
DOI:10.1021/jo401523m
- Guidance literature:
-
With
sodium;
at 100 ℃;