Hydrazinecarbothioyl chloride, trimethyl-

Base Information

• Chemical Name: Hydrazinecarbothioyl chloride, trimethyl-
• CAS No.: 38945-10-7
• Molecular Formula: C4H9ClN2S
• Molecular Weight: 152.648
• Mol file: 38945-10-7.mol

Synonyms:

Chemical Property of Hydrazinecarbothioyl chloride, trimethyl-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Hydrazinecarbothioyl chloride, trimethyl-

There total 1 articles about Hydrazinecarbothioyl chloride, trimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

thiophosgene (463-71-8) + Trimethylhydrazin (1741-01-1) → 2,3,3-Trimethyl(thiocarbazoyl)chlorid (38945-10-7)

Guidance literature:

With triethylamine; In dichloromethane;

Reference yield: 36.0%

2,3,3-Trimethyl(thiocarbazoyl)chlorid (38945-10-7) + 5,5-Diphenyl-2-thioxo-tetrahydro-4H-1,3-thiazin-4-on (76440-98-7) → 4-Oxo-5,5-diphenyl-2-thioxo-[1,3]thiazinane-3-carbothioic acid trimethylhydrazide (138020-09-4)

Guidance literature:

With triethylamine; In toluene; for 6h; Heating;

DOI:10.1002/ardp.2503241118

Reference yield: 21.0%

2,3,3-Trimethyl(thiocarbazoyl)chlorid (38945-10-7) + 5,5-Diphenyl-2-thioxo-tetrahydro-4H-1,3-thiazin-4-on (76440-98-7) → 2-(2,3,3-Trimethylthiocarbazoylmercapto)-5,5-diphenyl-5,6-dihydro-4H-1,3-thiazin-4-on (138020-15-2)

Guidance literature:

With triethylamine; In dichloromethane; at 40 ℃; for 6h;

DOI:10.1002/ardp.2503241118

upstream raw materials:

thiophosgene

Trimethylhydrazin

Downstream raw materials:

C₁₁H₁₆N₂O₂S₂

2-(2,3,3-Trimethylthiocarbazoylmercapto)-5,5-diphenyl-5,6-dihydro-4H-1,3-thiazin-4-on

4-Oxo-5,5-diphenyl-2-thioxo-[1,3]thiazinane-3-carbothioic acid trimethylhydrazide