Technology Process of Benzene, 1-hexyl-3,5-dimethoxy-
There total 7 articles about Benzene, 1-hexyl-3,5-dimethoxy- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen; acetic acid;
In
methanol;
for 24h;
under 1485.65 Torr;
DOI:10.1021/acs.jmedchem.1c00561
- Guidance literature:
-
With
sulfuric acid; hydrogen;
palladium on activated charcoal;
In
ethyl acetate;
for 4h;
under 2942.03 Torr;
Yield given;
Ambient temperature;
DOI:10.1016/S0031-9422(00)80159-4
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 89 percent / (COCl)2 / benzene / 2 h, room t., 1 h, reflux
2: 70 percent / NaOAc, H2 / 10percent Pd-C / 2427.2 Torr / 1h, then 60 degC, overnight
3: 1.) Mg; MeI / diethyl ether / 1.) 3 h, reflux; 2.) 1 h, reflux
4: hydrogen, conc. H2SO4 / 10percent Pd-C / ethyl acetate / 4 h / 2942.03 Torr / Ambient temperature
With
oxalyl dichloride; sulfuric acid; hydrogen; sodium acetate; magnesium; methyl iodide;
palladium on activated charcoal;
In
diethyl ether; ethyl acetate; benzene;
DOI:10.1016/S0031-9422(00)80159-4