Technology Process of 7-Methylnonanoic acid
There total 8 articles about 7-Methylnonanoic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
6-bromohexanoic acid;
With
1-methyl-pyrrolidin-2-one; tert-butylmagnesium chloride;
In
tetrahydrofuran;
at -78 ℃;
for 0.166667h;
Inert atmosphere;
s-butylmagnesium chloride;
With
buta-1,3-diene; nickel dichloride;
In
tetrahydrofuran;
for 1h;
under 760.051 Torr;
Inert atmosphere;
Cooling with ice;
DOI:10.1002/chem.201204222
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 50 percent / diethyl ether / 4 h / Heating
2: 53 percent / HCl / 2.5 h / Heating
3: 1.) hydrazine hydrate, 2.) NaOH, H2O / 1.) diethyleneglycol, reflux, 1 h, 2.) diethyleneglycol, a) reflux, 2 h, b) 195 to 200 deg C, 2 h
With
hydrogenchloride; sodium hydroxide; water; hydrazine hydrate;
In
diethyl ether;
