2,2,4,4,6,6,8,8-octakis(2,2,2-trifluoroethoxy)-1,3,5,7,2lambda~5~,4lambda~5~,6lambda~5~,8lambda~5~-tetrazatetraphosphocine

Base Information

• Chemical Name: 2,2,4,4,6,6,8,8-octakis(2,2,2-trifluoroethoxy)-1,3,5,7,2lambda~5~,4lambda~5~,6lambda~5~,8lambda~5~-tetrazatetraphosphocine
• CAS No.: 562-88-9
• Molecular Formula: C16H16F24N4O8P4
• Molecular Weight: 972.177
• Mol file: 562-88-9.mol

Synonyms:

Chemical Property of 2,2,4,4,6,6,8,8-octakis(2,2,2-trifluoroethoxy)-1,3,5,7,2lambda~5~,4lambda~5~,6lambda~5~,8lambda~5~-tetrazatetraphosphocine

Chemical Property:

• Vapor Pressure: 3.59E-08mmHg at 25°C
• Boiling Point: 459°Cat760mmHg
• Flash Point: 231.4°C
• Density: 1.85g/cm³

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,2,4,4,6,6,8,8-octakis(2,2,2-trifluoroethoxy)-1,3,5,7,2lambda~5~,4lambda~5~,6lambda~5~,8lambda~5~-tetrazatetraphosphocine

There total 6 articles about 2,2,4,4,6,6,8,8-octakis(2,2,2-trifluoroethoxy)-1,3,5,7,2lambda~5~,4lambda~5~,6lambda~5~,8lambda~5~-tetrazatetraphosphocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium 2,2,2-trifluoroethanolate (420-87-1) → Octakis-(2,2,2-trifluorethoxy)-cyclotetraphosphazen (562-88-9)

Guidance literature:

With octachlorocyclotetraphosphazene; In tetrahydrofuran;

Reference yield:

sodium 2,2,2-trifluoroethanolate (420-87-1) → Octakis-(2,2,2-trifluorethoxy)-cyclotetraphosphazen (562-88-9) + C12H12F18N4O8P4(2-)*2Na(1+) + C14H14F21N4O8P4(1-)*Na(1+)

Guidance literature:

With 1,1,3,3,5,5,7,7-octaphenoxycyclotetraphosphazatetraene; In tetrahydrofuran; at 66 ℃; for 72h; Inert atmosphere;

DOI:10.1039/c1dt11606a

Reference yield:

2,2,2-trifluoroethanol (75-89-8) → Octakis-(2,2,2-trifluorethoxy)-cyclotetraphosphazen (562-88-9)

Guidance literature:

Multistep reaction; (i) Na, Et₂O, (ii) (NPCl₂)4;

DOI:10.1021/ja00756a023

upstream raw materials:

2,2,2-trifluoroethanol

sodium 2,2,2-trifluoroethanolate

(N₃P₃Cl₄)(N₄P₄Cl₇)(C₅H₄)Fe(C₅H₅)

(N₃P₃Cl₄)(N₄P₄Cl₇)(C₅H₄)Fe(C₅H₄Cl)

Refernces

• 1、 Swamy, K. C. Kumara,Krishnamurthy, S. S.,Vasudeva Murthy, A. R.,Shaw, R. A.,Woods, M.. "Studies of Phosphazenes: Part 29 - Reaction of Octachlorocyclotetraphosphazene with Sodium 2,2,2-Trifluoroethoxide". . p. 1004 - 1011. Retrieved 2007/10/02.
• 2、 Evans,Allcock. "The partial aminolysis of (NPF2)3,4". . p. 2342 - 2345. Retrieved 2007/10/05.