1,1'-(Oxybisethylene)biscyclohexane

Base Information

• Chemical Name: 1,1'-(Oxybisethylene)biscyclohexane
• CAS No.: 55255-91-9
• Molecular Formula: C16H30O
• Molecular Weight: 238.414
• Hs Code.: 2909209000
• Mol file: 55255-91-9.mol

Synonyms:Bis-(2-cyclohexyl-aethyl)-aether;bis-(2-cyclohexyl-ethyl)-ether;Cyclohexane,1'-(oxydi-2,1-ethanediyl)bis;[2-(2-Cyclohexylethoxy)ethyl]cyclohexane;Cyclohexane, 1,1‘-(oxydi-2,1-ethanediyl)bis-;Cyclohexane,1,1'-(oxydi-2,1-ethanediyl)bis;1,1'-(oxydi-2,1-ethanediyl)bis-cyclohexane;

Chemical Property of 1,1'-(Oxybisethylene)biscyclohexane

Chemical Property:

• Boiling Point: 330°Cat760mmHg
• Flash Point: 138.2°C
• PSA: 9.23000
• Density: 0.896g/cm³
• LogP: 4.94380

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,1'-(Oxybisethylene)biscyclohexane

There total 4 articles about 1,1'-(Oxybisethylene)biscyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-phenethoxybenzene (40515-89-7) → cyclohexyl ethyl ether (932-92-3) + cyclohexylethan-1-ol (4442-79-9) + cyclohexane (110-82-7,25012-93-5) + bis-(2-cyclohexyl-ethyl)-ether (55255-91-9) + cyclohexanol (108-93-0)

Guidance literature:

With hydrogen; platinum(II) chloride; In ethanol; at 60 ℃; for 6h; under 750.075 - 1500.15 Torr;

Reference yield:

di(2-phenylethyl) ether (2396-53-4) → bis-(2-cyclohexyl-ethyl)-ether (55255-91-9)

Guidance literature:

With kieselguhr; nickel; at 140 ℃; under 25742.8 Torr; Hydrogenation;

Reference yield:

2-phenylethanol (60-12-8) → bis-(2-cyclohexyl-ethyl)-ether (55255-91-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuric acid

2: nickel /kieselguhr / 140 °C / 25742.8 Torr / Hydrogenation

With kieselguhr; sulfuric acid; nickel;

upstream raw materials:

di(2-phenylethyl) ether

2-phenylethanol

2-phenethoxybenzene

Downstream raw materials:

1-bromo-2-cyclohexylethane

Refernces