2-Butynoic acid, 4-hydroxy-4-phenyl-

Base Information

• Chemical Name: 2-Butynoic acid, 4-hydroxy-4-phenyl-
• CAS No.: 62952-24-3
• Molecular Formula: C10H8O3
• Molecular Weight: 176.172
• Mol file: 62952-24-3.mol

Synonyms:

Chemical Property of 2-Butynoic acid, 4-hydroxy-4-phenyl-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Butynoic acid, 4-hydroxy-4-phenyl-

There total 1 articles about 2-Butynoic acid, 4-hydroxy-4-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon dioxide (124-38-9,18923-20-1) → 4-hydroxy-4-phenyl-but-2-ynoic acid (62952-24-3)

Guidance literature:

With toluene;

DOI:10.1039/jr9490000118

Reference yield: 100.0%

4-hydroxy-4-phenyl-but-2-ynoic acid (62952-24-3) → 1-Phenyl-2-propyn-1-ol (4187-87-5)

Guidance literature:

With copper; In acetonitrile; for 3h; Heating;

DOI:10.1055/s-0030-1258487

Reference yield: 97.0%

4-hydroxy-4-phenyl-but-2-ynoic acid (62952-24-3) → 5-phenyl-2,5-dihydrofuran-2-one (53138-45-7)

Guidance literature:

With hydrogen; 5% Pd/CaCO3; In ethyl acetate; for 0.5h;

DOI:10.1021/jo00346a016

upstream raw materials:

carbon dioxide

Downstream raw materials:

3,4-dioxo-4-phenyl-butyric acid

5-phenyl-2,5-dihydrofuran-2-one

5-phenyl-3H-furan-2-one

cis-2,3-epoxy-4-phenylbutanoic acid γ-lactone