1,2-Dicyclohexylethane

Base Information

• Chemical Name: 1,2-Dicyclohexylethane
• CAS No.: 3321-50-4
• Molecular Formula: C14H26
• Molecular Weight: 194.36
• Hs Code.: 2902199090
• European Community (EC) Number: 222-032-6
• NSC Number: 94064
• DSSTox Substance ID: DTXSID70186860
• Nikkaji Number: J110.631G
• Wikidata: Q83058272
• Mol file: 3321-50-4.mol

Synonyms:1,2-Dicyclohexylethane;3321-50-4;2-cyclohexylethylcyclohexane;Ethane, 1,2-dicyclohexyl-;Cyclohexane, 1,1'-(1,2-ethanediyl)bis-;EINECS 222-032-6;(2-Cyclohexylethyl)cyclohexane;NSC94064;Ethane,2-dicyclohexyl-;1,2-dicyclohexyl-ethane;NCIOpen2_001466;1,2-Dicyclohexylethane, 97%;(2-Cyclohexylethyl)cyclohexane #;DTXSID70186860;MFCD00013768;NSC 94064;NSC-94064;AKOS006280590;Cyclohexane,1'-(1,2-ethanediyl)bis-;FT-0606391

Chemical Property of 1,2-Dicyclohexylethane

Chemical Property:

• Vapor Pressure: 0.0103mmHg at 25°C
• Melting Point: 11.5°C
• Refractive Index: 1.465
• Boiling Point: 272.2 °C at 760 mmHg
• Flash Point: 106.7 °C
• PSA: 0.00000
• Density: 0.858 g/cm³
• LogP: 4.92720
• XLogP3: 6.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 3
• Exact Mass: 194.203450829
• Heavy Atom Count: 14
• Complexity: 120

Purity/Quality:

99% ^*data from raw suppliers

1,2-Dicyclohexylethane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCC(CC1)CCC2CCCCC2

Technology Process of 1,2-Dicyclohexylethane

There total 44 articles about 1,2-Dicyclohexylethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

stilbene (588-59-0) → 1,2-dicyclohexylethane (3321-50-4)

Guidance literature:

With 10% Pt/activated carbon; isopropyl alcohol; In water; at 100 ℃; for 24h; Sealed tube;

DOI:10.1002/adsc.201500263

Reference yield: 89.0%

phenyl benzyl ketone (451-40-1) → 1,2-dicyclohexylethane (3321-50-4)

Guidance literature:

With rhodium(III) chloride; hydrogen; In 2,2,2-trifluoroethanol; at 100 ℃; for 10h; under 37503.8 Torr; chemoselective reaction;

DOI:10.1039/d1cy01504d

Reference yield: 88.0%

1,1'-(1,2-ethanediyl)bisbenzene (103-29-7) → (2-cyclohexyl-ethyl)-benzene (1603-61-8) + 1,2-dicyclohexylethane (3321-50-4)

Guidance literature:

With MmNi_3.5Co_0.7Al_0.8H₄; at 160 ℃; for 3h; under 3677.5 Torr;

DOI:10.1246/cl.1994.431

upstream raw materials:

1,2-Diphenylethanol

di(1-cyclohexen-1-yl)ethyne

2-hydroxy-2-phenylacetophenone

1,1'-(1,2-ethanediyl)bisbenzene

Downstream raw materials:

1,1'-(1,2-ethanediyl)bisbenzene

phenanthrene

Refernces

• 1、 Cao, Meifang,Chen, Bo,He, Chengzhi,Ouyang, Xinping,Qian, Yong,Qiu, Xueqing. "Fabricating nickel phyllosilicate-like nanosheets to prepare a defect-rich catalyst for the one-pot conversion of lignin into hydrocarbons under mild conditions". supporting information. p. 846 - 857. Retrieved 2022/02/09.
• 2、 Bartling, Stephan,Chakrabortty, Soumyadeep,De Vries, Johannes G.,Kamer, Paul C. J.,Lund, Henrik,Müller, Bernd H.,Rockstroh, Nils. "The solvent determines the product in the hydrogenation of aromatic ketones using unligated RhCl3as catalyst precursor". . p. 7608 - 7616. Retrieved 2021/12/13.