Technology Process of (Z)-1-Bromo-5-decene
There total 14 articles about (Z)-1-Bromo-5-decene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
bromine; triethylphosphine;
In
tetrachloromethane;
1.) 15 deg C, 1h, 2.) RT, 15 h;
- Guidance literature:
-
With
lithium bromide;
In
acetone;
at 40 ℃;
for 3h;
DOI:10.1007/bf02505687
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 95 percent / diisobutylaluminum hydride / diethyl ether; toluene / 1.5 h / -10 °C
2: pyridine / 15 h / -10 °C
3: Zn, sodium iodide / bis-(2-methoxy-ethyl) ether / 1.5 h / Heating
4: 10percent aq. hydrochloric acid / acetone / 6 h / Ambient temperature
5: diisobutylaluminum hydride / diethyl ether; toluene / 1.5 h / -10 °C
6: 87 percent / trifenylphosphine, bromine / CCl4 / 1.) 15 deg C, 1h, 2.) RT, 15 h
With
pyridine; hydrogenchloride; bromine; diisobutylaluminium hydride; sodium iodide; zinc; triethylphosphine;
In
tetrachloromethane; diethyl ether; diethylene glycol dimethyl ether; acetone; toluene;
