4-DIMETHYLAMINOBENZYLAMINE

Base Information

• Chemical Name: 4-DIMETHYLAMINOBENZYLAMINE
• CAS No.: 19293-58-4
• Molecular Formula: C9H14N2
• Molecular Weight: 150.224
• Hs Code.: 2921590090
• Mol file: 19293-58-4.mol

Synonyms:Toluene-a,4-diamine, N4,N4-dimethyl-(6CI,7CI,8CI);(4-Aminomethylphenyl)dimethylamine;4-(Aminomethyl)-N,N-dimethylaniline;4-(Dimethylamino)benzenemethanamine;4-(N,N-Dimethylamino)benzylamine;4-Dimethylaminobenzylamine;[[4-(Dimethylamino)phenyl]methyl]amine;p-(N,N-Dimethylamino)benzylamine;p-Dimethylaminobenzylamine;

Chemical Property of 4-DIMETHYLAMINOBENZYLAMINE

Chemical Property:

• Vapor Pressure: 0.383mmHg at 25°C
• Melting Point: 169-171 °C
• Refractive Index: 1.472
• Boiling Point: 260 °C at 760 mmHg
• PKA: 9.70±0.10(Predicted)
• Flash Point: 98.6 °C
• PSA: 29.26000
• Density: 1.019 g/cm³
• LogP: 1.91160

Purity/Quality:

99% ^*data from raw suppliers

4-Dimethylaminobenzylamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s): CXi
• Hazard Codes: C,Xi

MSDS Files:

Useful:

• Uses: 4-Dimethylaminobenzylamine is an Inhibition of rabbit liver monoamine oxidase.

Technology Process of 4-DIMETHYLAMINOBENZYLAMINE

There total 18 articles about 4-DIMETHYLAMINOBENZYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.9%

4-dimethylamino-benzaldehyde (100-10-7) → (4-aminomethylphenyl)dimethylamine (19293-58-4)

Guidance literature:

With ammonium hydroxide; hydrogen; In ethanol; at 130 ℃; for 12h; under 7500.75 Torr; Autoclave;

DOI:10.1016/j.jcat.2019.01.004

Reference yield: 98.0%

→ (4-aminomethylphenyl)dimethylamine (19293-58-4)

Guidance literature:

With ammonia; hydrogen; In methanol; at 90 ℃; for 4h; under 15001.5 Torr; Autoclave;

Reference yield: 95.0%

4,4'-(1E,1'E)-hydrazine-1,2-diylidenebis(methan-1-yl-1-ylidene)bis(N,N-dimethylaniline) (108026-63-7) → (4-aminomethylphenyl)dimethylamine (19293-58-4)

Guidance literature:

With methanesulfonic acid; zinc; In tetrahydrofuran; at 25 ℃; for 8h;

DOI:10.1016/S0040-4039(01)00178-2

upstream raw materials:

4-dimethylaminobenzaldehyde oxime

2-(4-(dimethylamino)benzyl)isoindoline-1,3-dione

4-dimethylamino-benzaldehyde

4-dimethylamino-benzaldehyde phenylhydrazone

Downstream raw materials:

(2R)-N-(4-dimethylaminobenzyl)-3-cyclohexylmethylthio-2-t-butoxycarbonyl-aminopropanamide

5-(8-(4-(1,4'-bipiperidine-1'-carbonyl)phenylamino)imidazo[1,2-a]pyridin-5-yl)isoindolin-1-one

C₁₅H₁₇N₃O

Refernces

• 1、 Beller, Matthias,Chandrashekhar, Vishwas G.,Gawande, Manoj B.,Jagadeesh, Rajenahally V.,Kalevaru, Narayana V.,Kamer, Paul C. J.,Senthamarai, Thirusangumurugan,Zbo?il, Radek. "Ultra-small cobalt nanoparticles from molecularly-defined Co-salen complexes for catalytic synthesis of amines". . p. 2973 - 2981. Retrieved 2020/03/27.
• 2、 Cui, Zhibing,Liu, Jianguo,Liu, Qiying,Ma, Longlong,Singh, Thishana,Wang, Chenguang,Wang, Nan,Zhu, Yuting. "Facile synthesis of controllable graphene-co-shelled reusable Ni/NiO nanoparticles and their application in the synthesis of amines under mild conditions". supporting information. p. 7387 - 7397. Retrieved 2020/11/19.