Methyl(α-methylbenzyl)dichlorosilane

Base Information

• Chemical Name: Methyl(α-methylbenzyl)dichlorosilane
• CAS No.: 7282-39-5
• Molecular Formula: C9H12Cl2Si
• Molecular Weight: 219.186
• Mol file: 7282-39-5.mol

Synonyms:(1-phenylethyl) methyldichlorosilane;dichloro-methyl-(1-phenyl-ethyl)-silane;methyl(1-phenylethyl)dichlorosilane;Silane,dichloromethyl(1-phenylethyl);(1-Phenyl-ethyl)-methyl-dichlorsilan;Dichlor-methyl-(1-phenyl-aethyl)-silan;

Chemical Property of Methyl(α-methylbenzyl)dichlorosilane

Chemical Property:

• PSA: 0.00000
• LogP: 3.19300

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl(α-methylbenzyl)dichlorosilane

There total 4 articles about Methyl(α-methylbenzyl)dichlorosilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

Dichloromethylsilane (75-54-7) + styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) → (1-phenyl-ethyl)methyldichlorosilane (7282-39-5)

Guidance literature:

With trans-dichlorobis(triphenylphosphine)platinum(II); regiospecific reaction;

DOI:10.1134/S1070363214020200

Reference yield: 14.7%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) → (1-phenyl-ethyl)methyldichlorosilane (7282-39-5) + monophenethyldichlorosilane (68704-60-9)

Guidance literature:

platinum;

Reference yield:

Dichloromethylsilane (75-54-7) + styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) → (2-phenylethyl)methyldichlorosilane (772-65-6) + (1-phenyl-ethyl)methyldichlorosilane (7282-39-5)

Guidance literature:

dihydrogen hexachloroplatinate; at 20 ℃; Product distribution; Kinetics; other catalysts, other temperatures;

upstream raw materials:

Dichloromethylsilane

styrene

Downstream raw materials:

1,1,2,3,3-pentamethyl-1,3-diphenyl-2-(1-phenyl-ethyl)trisilane

α-methylbenzyl(trimethyl)silane

Refernces

• 1、 Li, Laiming,Li, Youxin,Assefa, Aschenaki,Bao, James J.. "Preparation, characterization and evaluation of a series of heterogeneous platinum catalysts immobilized on magnetic silica with different acid ligands". . p. 779 - 787. Retrieved 2019/08/12.
• 2、 -. "SATURATED N-HETEROCYCLIC CARBENE-LIGAND METAL COMPLEX DERIVATIVES, PREPARING METHOD THEREOF, AND PREPARING METHOD OF SILANE COMPOUND BY HYDROSILYLATION REACTION USING THE SAME AS CATALYST". Page/Page column 18-19. . Retrieved 2011/07/30.