(3-Chloropropyl)ethoxydimethylsilane

Base Information

• Chemical Name: (3-Chloropropyl)ethoxydimethylsilane
• CAS No.: 13508-63-9
• Molecular Formula: C7H17 Cl O Si
• Molecular Weight: 180.75
• Hs Code.: 2931900090
• European Community (EC) Number: 236-837-5
• UNII: 9DZ4XF983L
• DSSTox Substance ID: DTXSID40159243
• Nikkaji Number: J241.158J
• Wikidata: Q83027560
• Mol file: 13508-63-9.mol

Synonyms:13508-63-9;(3-Chloropropyl)ethoxydimethylsilane;(3-Chloropropyl)(ethoxy)dimethylsilane;3-chloropropyl-ethoxy-dimethylsilane;3-chloropropyldimethylethoxysilane;Silane, (3-chloropropyl)ethoxydimethyl-;9DZ4XF983L;EINECS 236-837-5;C7H17ClOSi;C7-H17-Cl-O-Si;UNII-9DZ4XF983L;SCHEMBL56265;chloropropyldimethylethoxysilane;DTXSID40159243;MFCD09953850;AKOS006283762;1-Dimethyl(3-chloropropyl)silyloxyethane;(3-Chloropropyl)(ethoxy)dimethylsilane #;.GAMMA.-CHLOROPROPYLETHOXYLDIMETHYLSILANE;(.GAMMA.-CHLOROPROPYL)ETHOXYDIMETHYLSILANE;A887755

Chemical Property of (3-Chloropropyl)ethoxydimethylsilane

Chemical Property:

• Vapor Pressure: 2.23mmHg at 25°C
• Refractive Index: 1.427
• Boiling Point: 167.6°Cat760mmHg
• Flash Point: 47.6°C
• PSA: 9.23000
• Density: 0.914g/cm³
• LogP: 2.85690
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 5
• Exact Mass: 180.0737194
• Heavy Atom Count: 10
• Complexity: 85.7

Purity/Quality:

98%Min ^*data from raw suppliers

3-CHLOROPROPYLDIMETHYLETHOXYSILANE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCO[Si](C)(C)CCCCl

Technology Process of (3-Chloropropyl)ethoxydimethylsilane

There total 8 articles about (3-Chloropropyl)ethoxydimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

ethanol (64-17-5) + (3-chloropropyl)dimethylchlorosilane (10605-40-0) → chloropropyl(dimethyl)ethoxysilane (13508-63-9)

Guidance literature:

for 5h; Product distribution / selectivity; Heating / reflux;

Reference yield: 100.0%

ethanol (64-17-5) + 6-chloro-3,3-dimethyl-3-silahex-1-ene (88820-71-7) → chloropropyl(dimethyl)ethoxysilane (13508-63-9)

Guidance literature:

With hydrogenchloride; chlorobis(cyclooctene)rhodium(I) dimer; In 1,4-dioxane; chloroform; at 20 ℃; for 2h;

DOI:10.1021/ol701909e

Reference yield:

dimethyl(ethoxy)silane (14857-34-2) + 3-chloroprop-1-ene (107-05-1) → dimethyl chloro ethoxy silane (1825-69-0) + me2(n-pr)Si(Oet) (18387-29-6) + diethoxy dimethylsilane (78-62-6) + chloropropyl(dimethyl)ethoxysilane (13508-63-9) + (3-chloropropyl)dimethylchlorosilane (10605-40-0)

Guidance literature:

dimethyl(ethoxy)silane; ruthenium trichloride; In toluene; at 20 - 80 ℃; Under N₂ atmosphere;

3-chloroprop-1-ene; In toluene; at 80 ℃; for 1h; Under N₂ atmosphere;

upstream raw materials:

ethanol

(3-chloropropyl)dimethylchlorosilane

6-chloro-3,3-dimethyl-3-silahex-1-ene

C₅H₁₂Cl₂Si

Downstream raw materials:

1,3-bis(3-aminopropyl)-1,1,3,3-tetramethyldisiloxane

1,3-bis<3-chloropropyl>-1,1,3,3-tetramethyldisiloxane

chloropropyl dimethylsilanol

γ-chloropropylmethoxydimethylsilane

Refernces

• 1、 -. "Method for obtaining polysulphide monoorganoxysilanes". Page/Page column 8-9. . Retrieved 2011/05/08.
• 2、 -. "PROCESS FOR THE PREPARATION OF HALOALKYLALKOXYSILANCS AND HALOALKYLHALOSILANES". Page/Page column 13-14. . Retrieved 2009/10/22.