1-Butanesulfonamide, 1,1,2,2,3,3,4,4,4-nonafluoro-N-(2-hydroxyethyl)-N-methyl-

Base Information

• Chemical Name: 1-Butanesulfonamide, 1,1,2,2,3,3,4,4,4-nonafluoro-N-(2-hydroxyethyl)-N-methyl-
• CAS No.: 34454-97-2
• Molecular Formula: C7H8 F9 N O3 S
• Molecular Weight: 357.197
• Hs Code.: 2935009090
• European Community (EC) Number: 252-043-1
• UNII: KY6T23E87F
• DSSTox Substance ID: DTXSID0067848
• Nikkaji Number: J250.898B
• Wikidata: Q81994505
• Mol file: 34454-97-2.mol

Synonyms:C4F9SO2N(CH3)CH2CH2OH;N-methyl perfluorobutane sulfonamidoethanol

Chemical Property of 1-Butanesulfonamide, 1,1,2,2,3,3,4,4,4-nonafluoro-N-(2-hydroxyethyl)-N-methyl-

Chemical Property:

• Vapor Pressure: 0.00425mmHg at 25°C
• Melting Point: 57 °C
• Boiling Point: 247.2°Cat760mmHg
• PKA: 14.06±0.10(Predicted)
• Flash Point: 103.3°C
• PSA: 65.99000
• Density: 1.63g/cm³
• LogP: 2.74680
• Storage Temp.: Hygroscopic, Refrigerator, under inert atmosphere
• Solubility.: Acetone (Slightly), Methanol (Slightly)
• Water Solubility.: 141mg/L at 23℃
• XLogP3: 2.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 13
• Rotatable Bond Count: 6
• Exact Mass: 357.00811775
• Heavy Atom Count: 21
• Complexity: 467

Purity/Quality:

99.9% ^*data from raw suppliers

1,1,2,2,3,3,4,4,4-Nonafluoro-N-(2-hydroxyethyl)-N-methyl-1-butanesulfonamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(CCO)S(=O)(=O)C(C(C(C(F)(F)F)(F)F)(F)F)(F)F
• Uses: 1,1,2,2,3,3,4,4,4-Nonafluoro-N-(2-hydroxyethyl)-N-methyl-1-butanesulfonamide is derived from Nonafluoro-1-butanesulfonyl Fluoride (N649320), which is a useful perfluorinated compound (PFC) used in organic synthesis.

Technology Process of 1-Butanesulfonamide, 1,1,2,2,3,3,4,4,4-nonafluoro-N-(2-hydroxyethyl)-N-methyl-

There total 2 articles about 1-Butanesulfonamide, 1,1,2,2,3,3,4,4,4-nonafluoro-N-(2-hydroxyethyl)-N-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[1,3]-dioxolan-2-one (96-49-1) + N-methyl-perfluorobutane-1-sulfonamide (68298-12-4) → N-methyl-1,1,2,2,3,3,4,4-nonafluoro-N-(2-hydroxyethyl)butane-1-sulphonamide (34454-97-2)

Guidance literature:

With triethylamine; at 200 ℃;

Reference yield:

→ N-methyl-1,1,2,2,3,3,4,4-nonafluoro-N-(2-hydroxyethyl)butane-1-sulphonamide (34454-97-2)

Guidance literature:

sek.Sulfonamid, Ethylencarbonat;

Reference yield: 99.8%

N-methyl-1,1,2,2,3,3,4,4-nonafluoro-N-(2-hydroxyethyl)butane-1-sulphonamide (34454-97-2) + acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) → (N-methylperfluorobutylsulfonamido)ethyl acrylate (67584-55-8)

Guidance literature:

With sodium methylate; hydroquinone; at 74 - 76 ℃; for 10h;

upstream raw materials:

[1,3]-dioxolan-2-one

N-methyl-perfluorobutane-1-sulfonamide

Downstream raw materials:

(N-methylperfluorobutylsulfonamido)ethyl acrylate

C₂₂H₁₈F₉N₃O₅S

C₄F₉SO₂N(CH₃)CH₂CH₂OB(C₆H₅)2

C₄F₉SO₂N(CH₃)CH₂CH₂OB(C₆H₅)N(CH₃)2

Refernces

• 1、 -. "Functional fluorescent dyes". Page 8. . Retrieved 2008/06/13.