NAPHTHALEN-1-YL-PROPYLAMINE

Base Information

• Chemical Name: NAPHTHALEN-1-YL-PROPYLAMINE
• CAS No.: 607-60-3
• Molecular Formula: C13H15N
• Molecular Weight: 185.2649
• Mol file: 607-60-3.mol

Synonyms:1-Naphthalenamine, N-propyl-;Naphthalen-1-ylpropylamine;N-propyl-1-naphthalenamine;N-n-Propyl-1-naphthylamin;N-Allyldihydro-1-naphthylamin;

Chemical Property of NAPHTHALEN-1-YL-PROPYLAMINE

Chemical Property:

• Vapor Pressure: 0.000279mmHg at 25°C
• Boiling Point: 322.4°Cat760mmHg
• Flash Point: 157.1°C
• PSA: 12.03000
• Density: 1.052g/cm³
• LogP: 3.73470

Purity/Quality:

98%min ^*data from raw suppliers

N-propylnaphthalen-1-amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of NAPHTHALEN-1-YL-PROPYLAMINE

There total 6 articles about NAPHTHALEN-1-YL-PROPYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

propylamine (107-10-8,42939-71-9) + 1-Iodonaphthalene (90-14-2) → N-propylnaphthalen-1-amine (607-60-3)

Guidance literature:

With 1,2-ethanedione dioxime; tetrabutylammomium bromide; copper(I) bromide; sodium hydroxide; In water; at 100 ℃; for 24h; Inert atmosphere; sealed tube;

DOI:10.1039/c002172e

Reference yield: 60.0%

1-amino-naphthalene (134-32-7) + propyl bromide (106-94-5) → N-propylnaphthalen-1-amine (607-60-3)

Guidance literature:

In methanol; Reflux;

DOI:10.1016/j.tetlet.2009.05.055

Reference yield: 27.0%

N-(2-propenyl)-1-naphthylamine (22950-23-8) → N-propylnaphthalen-1-amine (607-60-3) + N-(1-naphthyl)pyrrolidine (82238-92-4)

Guidance literature:

With sodium tetrahydroborate; carbon monoxide; η⁶-C6H6BPh3^-Rh(COD)⁺; In dichloromethane; isopropyl alcohol; at 100 ℃; for 30h; under 26220 Torr;

DOI:10.1021/jo00038a019

upstream raw materials:

carbon monoxide

N-(2-propenyl)-1-naphthylamine

1-amino-naphthalene

propyl bromide

Refernces

• 1、 Raju, B. Rama,Garcia, Arlindo M. Fontes,Costa, A. Luísa S.,Coutinho, Paulo J.G.,Gon?alves, M. Sameiro T.. "Synthesis of new benzo[a]phenoxazinium probes possessing carboxylic ester, hydroxyl and amino functional groups: Photophysical studies in dry ethanol and conjugation with CdTe quantum dots". . p. 203 - 213. Retrieved 2014.
• 2、 Raju, B. Rama,Firmino, A. Daniela G.,Costa, A. Luísa S.,Coutinho, Paulo J.G.,Gon?alves, M. Sameiro T.. "Synthesis and photophysical properties of side-chain chlorinated benzo[a]phenoxazinium chlorides". . p. 2451 - 2461. Retrieved 2013/03/14.