Boranamine, 1,1-dichloro-N,N-diethyl-

Base Information

• Chemical Name: Boranamine, 1,1-dichloro-N,N-diethyl-
• CAS No.: 868-30-4
• Molecular Formula: C4H10BCl2N
• Molecular Weight: 153.847
• DSSTox Substance ID: DTXSID20416104
• Nikkaji Number: J3.231.661A
• Wikidata: Q82225274
• Mol file: 868-30-4.mol

Synonyms:Boranamine, 1,1-dichloro-N,N-diethyl-;diethylaminoboron dichloride;868-30-4;N,N-diethylaminodichloroborane;N,N-Diethyldichloroboraneamine;SCHEMBL8966916;DTXSID20416104;YYFUACSSDDWTEK-UHFFFAOYSA-N;InChI=1/C4H10BCl2N/c1-3-8(4-2)5(6)7/h3-4H2,1-2H

Chemical Property of Boranamine, 1,1-dichloro-N,N-diethyl-

Chemical Property:

• Vapor Pressure: 5.94mmHg at 25°C
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 153.0283349
• Heavy Atom Count: 8
• Complexity: 56

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: B(N(CC)CC)(Cl)Cl

Technology Process of Boranamine, 1,1-dichloro-N,N-diethyl-

There total 6 articles about Boranamine, 1,1-dichloro-N,N-diethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

diphenyl(diethylamino)borane (7397-50-4) + boron trichloride (10294-34-5) → diphenylboronchloride (3677-81-4) + Diethylaminodichloroborane (868-30-4)

Guidance literature:

distn. of BCl3 into (C6H5)2BN(C2H5)2 at -50°C; distn.;

DOI:10.1016/0022-328X(68)80063-4

Reference yield: 53.0%

tris(diethylamino)borane (867-97-0) → diethyl amine hydrochloride (660-68-4) + Diethylaminodichloroborane (868-30-4)

Guidance literature:

With HCl; In diethyl ether;

Reference yield:

boron trichloride (10294-34-5) + diethylamine (109-89-7) → triethylamine hydrochloride (554-68-7) + Diethylaminodichloroborane (868-30-4)

Guidance literature:

With triethylamine; In benzene; treatment of BCl3 with (C2H5)2NH at -78°C, then giving of triethylamine at room temp.; evapn, distn.;

DOI:10.1021/ja01523a019

upstream raw materials:

boron trichloride

diethylamine

tris(diethylamino)borane

diphenyl(diethylamino)borane

Downstream raw materials:

C₁₀H₁₉BClNO

Bis-triphenylsilyl-diaethylamino-boran

diethyl-diethylamino-borane

diphenyl(diethylamino)borane