Technology Process of 1H-Imidazolium,
4-[(2S)-2-(benzoylamino)-3-methoxy-3-oxopropyl]-1,3-dipropyl-,
bromide
There total 1 articles about 1H-Imidazolium,
4-[(2S)-2-(benzoylamino)-3-methoxy-3-oxopropyl]-1,3-dipropyl-,
bromide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
dichloromethane;
byproducts: H2O; (Ar); using Schlenk techniques; addn. of Ag2O (2.71 mmol) to soln. of (MeOCOCH(NHCOPh)CH2C3H2N2(n-Pr)2)Br (2.29 mmol) in abs. CH2Cl2 at room temp., stirring in the dark for 2 h (in some reactions addn. of molecular sieves and shaking); pptn., decanting, removal of solvent in vac., drying in vac., elem. anal.;
DOI:10.1016/j.jorganchem.2005.07.115
- Guidance literature:
-
In
dichloromethane;
byproducts: H2O; (Ar); using Schlenk techniques; addn. of Ag2O (0.52 equiv.) to soln. of (MeOCOCH(NHCOPh)CH2C3H2N2(n-Pr)2)Br in CH2Cl2, stirring in the dark for 2 h at ambient temp., addn. of 0.5 equiv. of Pd(MeCN)2Cl2 in abs. CH2Cl2; stirring for 1 h at room temp.; pptn., decanting, removal of solvent in vac., drying in vac.; as mixt. of diastereomers;
DOI:10.1016/j.jorganchem.2005.07.115
