Hexane, 1,6-dicyclohexyl-

Base Information

• Chemical Name: Hexane, 1,6-dicyclohexyl-
• CAS No.: 1610-23-7
• Molecular Formula: C18H34
• Molecular Weight: 250.4626
• Hs Code.: 2902199090
• DSSTox Substance ID: DTXSID90167050
• Nikkaji Number: J103.448K
• Wikidata: Q83036365
• Mol file: 1610-23-7.mol

Synonyms:1,6-Dicyclohexylhexane;Hexane, 1,6-dicyclohexyl-;6-cyclohexylhexylcyclohexane;1610-23-7;Cyclohexane, 1,1'-(1,6-hexanediyl)bis-;(6-Cyclohexylhexyl)cyclohexane #;DTXSID90167050;VBQJFJRTZSWYPK-UHFFFAOYSA-N

Chemical Property of Hexane, 1,6-dicyclohexyl-

Chemical Property:

• Melting Point: 8.6°C
• Refractive Index: 1.4750
• Boiling Point: 340.3°Cat760mmHg
• Flash Point: 149.2°C
• PSA: 0.00000
• Density: 0.856g/cm³
• LogP: 6.48760
• XLogP3: 9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 7
• Exact Mass: 250.266051085
• Heavy Atom Count: 18
• Complexity: 162

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCC(CC1)CCCCCCC2CCCCC2

Technology Process of Hexane, 1,6-dicyclohexyl-

There total 6 articles about Hexane, 1,6-dicyclohexyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.6%

1,4-dibenzoylbutane (3375-38-0) → 1-cyclohexyl-6-phenylhexane (1204165-13-8) + 1,6-diphenylhexane (1087-49-6) + 1,6-dicyclohexylhexane (1610-23-7)

Guidance literature:

With Raney Ni-Al alloy; water; potassium hydroxide; at 90 ℃; for 8h;

DOI:10.3184/030823409X12506792542783

Reference yield:

1,6-diphenylhexane (1087-49-6) → 1,6-dicyclohexylhexane (1610-23-7)

Guidance literature:

With nickel; methyl cyclohexane; at 180 ℃; under 88260.9 Torr; Hydrogenation;

DOI:10.1021/ja01155a055

Reference yield:

1-Bromo-3-phenylpropane (637-59-2) → 1,6-dicyclohexylhexane (1610-23-7)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium; diethyl ether

2: platinum; glacial acetic acid / Hydrogenation

With diethyl ether; sodium; acetic acid; platinum;

DOI:10.1021/ja01179a056

upstream raw materials:

1,6-diphenyl-hexa-1,3,5-triene

1,6-diphenylhexane

1-Bromo-3-phenylpropane

1,6-diphenyl-hexa-1,5-diene-3,4-diol

Downstream raw materials:

dodecafluoro-1,6-bis-undecafluorocyclohexyl-hexane

Refernces