4-N-DODECYLOXYNITROBENZENE

Base Information

• Chemical Name: 4-N-DODECYLOXYNITROBENZENE
• CAS No.: 65039-18-1
• Molecular Formula: C18H29 N O3
• Molecular Weight: 307.433
• Hs Code.: 2909309090
• Mol file: 65039-18-1.mol

Synonyms:4-Dodecyloxynitrobenzene;Lauryl 4-nitrophenyl ether; p-Dodecyloxynitrobenzene

Chemical Property of 4-N-DODECYLOXYNITROBENZENE

Chemical Property:

• Vapor Pressure: 6.11E-07mmHg at 25°C
• Melting Point: 51 °C
• Boiling Point: 220 °C / 20mmHg
• Flash Point: 149.1°C
• PSA: 55.05000
• Density: 1.001g/cm³
• LogP: 6.41770

Purity/Quality:

98%,99%, ^*data from raw suppliers

1-Dodecyloxy-4-nitrobenzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-N-DODECYLOXYNITROBENZENE

There total 7 articles about 4-N-DODECYLOXYNITROBENZENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + 1-dodecylbromide (143-15-7) → 4-dodecyloxy-1-nitrobenzene (65039-18-1)

Guidance literature:

With potassium carbonate; In acetone; at 60 ℃; for 5h; Inert atmosphere;

DOI:10.1021/ja302574b

Reference yield:

potassium 4-nitrophenolate (1124-31-8) + 1-dodecylbromide (143-15-7) → 4-dodecyloxy-1-nitrobenzene (65039-18-1)

Guidance literature:

With ethanol; zinc(II) chloride; at 180 ℃;

Reference yield:

dodecyloxybenzene (35021-68-2) → 4-dodecyloxy-1-nitrobenzene (65039-18-1)

Guidance literature:

With nitric acid; acetic acid;

DOI:10.1021/jacs.5b03396

upstream raw materials:

potassium 4-nitrophenolate

1-dodecylbromide

4-nitro-phenol

1-chlorododecane

Downstream raw materials:

(E)-4,4'-dimethylazobenzene

4-dodecyloxy-4'-(1-hydroxytriethylenglycol)azobenzene

C₄₄H₆₆N₄O₄

4-(dodecyloxy)-N-((4-(dodecyloxy)phenyl)carbamothioyl)benzamide

Refernces

• 1、 Hsu, Yuan?Chun,Wang, Chun?Yang,Hsiao, Pei?Chi,Cai, Yi-Hong,Lee, Gene?Hsiang,Lai, Chung K.. "Polarization effect in luminescent mesogenic BF2 complexes derived from heterocyclic benzothiazoles". . . Retrieved 2019/12/09.
• 2、 Yuan, Lin,Shen, Jie,Ye, Ruijuan,Chen, Feng,Zeng, Huaqiang. "Structurally simple trimesic amides as highly selective anion channels". supporting information. p. 4797 - 4800. Retrieved 2019/05/02.