Di(3,5,5-triMethylhexyl)aMine

Base Information

• Chemical Name: Di(3,5,5-triMethylhexyl)aMine
• CAS No.: 926-75-0
• Molecular Formula: C18H39N
• Molecular Weight: 269.514
• Mol file: 926-75-0.mol

Synonyms:Di-<3,5,5-trimethyl-hexyl)-amin;Diisononylamin;

Chemical Property of Di(3,5,5-triMethylhexyl)aMine

Chemical Property:

• PSA: 12.03000
• LogP: 5.89170
• Storage Temp.: Refrigerator

Purity/Quality:

99%, ^*data from raw suppliers

Di(3,5,5-trimethylhexyl)amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Di(3,5,5-triMethylhexyl)aMine is used in the preparation of N-nitrosoamines series.

Technology Process of Di(3,5,5-triMethylhexyl)aMine

There total 3 articles about Di(3,5,5-triMethylhexyl)aMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

3,5,5-trimethylhexanoic acid (3302-10-1) → 3,5,5-trimethylhexylamine (3378-63-0) + 3,5,5-trimethylhexanamide (90726-43-5) + bis(3,5,5-trimethylhexyl)amine (926-75-0)

Guidance literature:

3,5,5-trimethylhexanoic acid; With cyclopentyl methyl ether; ammonia; at 200 ℃; under 4500.45 Torr; Sealed tube; Green chemistry;

With cyclopentyl methyl ether; ammonia; hydrogen; at 200 ℃; for 6.5h; under 42004.2 Torr; Cooling with ice; Green chemistry;

DOI:10.1039/d0gc01441a

Reference yield:

(3,5,5-trimethyl-hexyl)-(3,5,5-trimethyl-hexylidene)-amine (3378-76-5) → bis(3,5,5-trimethylhexyl)amine (926-75-0)

Guidance literature:

With hydrogen;

DOI:10.1039/j39660001384

Reference yield:

3,5,5-trimethylhexylamine (3378-63-0) → bis(3,5,5-trimethylhexyl)amine (926-75-0)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. Na₂S₂O₈, AgNO₃, NaOH

2: H₂

With sodium hydroxide; sodium persulfate; hydrogen; silver nitrate;

DOI:10.1039/j39660001384

upstream raw materials:

(3,5,5-trimethyl-hexyl)-(3,5,5-trimethyl-hexylidene)-amine

3,5,5-trimethylhexylamine

3,5,5-trimethylhexanoic acid

Downstream raw materials:

3-(2,4-Dimethyl-phenyl)-1,1-bis-(3,5,5-trimethyl-hexyl)-urea

Refernces