Isopyrodelphinine

Base Information

• Chemical Name: Isopyrodelphinine
• CAS No.: 60158-63-6
• Molecular Formula: C₃₂H₄₁NO₈
• Molecular Weight: 567.679
• Mol file: 60158-63-6.mol

Synonyms:

Chemical Property of Isopyrodelphinine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Isopyrodelphinine

There total 2 articles about Isopyrodelphinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

delphinine (561-07-9) → isopyrodelphinine (60158-63-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 220 mg / 0.12 h / 230 - 240 °C / 0.01 Torr

2: 146 mg / TsOH / 1.) RT, 30 min, 2.) 70-80 deg C, 1 h

With toluene-4-sulfonic acid;

DOI:10.1021/jo00148a012

Reference yield:

pyrodelphinine (60050-12-6) + acetic acid (64-19-7,77671-22-8) → isopyrodelphinine (60158-63-6)

Guidance literature:

With toluene-4-sulfonic acid; 1.) RT, 30 min, 2.) 70-80 deg C, 1 h;

DOI:10.1021/jo00148a012

Reference yield:

isopyrodelphinine (60158-63-6) → 16-demethoxydelphinine (83705-17-3)

Guidance literature:

With hydrogen; palladium on activated charcoal; In acetic acid; for 42h; under 2660 Torr;

DOI:10.1021/jo00148a012

upstream raw materials:

pyrodelphinine

acetic acid

delphinine

Downstream raw materials:

16-demethoxydelphinine

16-demethoxypyrodelphinine

Refernces