Technology Process of 16-demethoxydelphinine
There total 3 articles about 16-demethoxydelphinine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
acetic acid;
for 42h;
under 2660 Torr;
DOI:10.1021/jo00148a012
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 146 mg / TsOH / 1.) RT, 30 min, 2.) 70-80 deg C, 1 h
2: 242 mg / H2 / 10percent Pd/C / acetic acid / 42 h / 2660 Torr
With
hydrogen; toluene-4-sulfonic acid;
palladium on activated charcoal;
In
acetic acid;
DOI:10.1021/jo00148a012
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 220 mg / 0.12 h / 230 - 240 °C / 0.01 Torr
2: 146 mg / TsOH / 1.) RT, 30 min, 2.) 70-80 deg C, 1 h
3: 242 mg / H2 / 10percent Pd/C / acetic acid / 42 h / 2660 Torr
With
hydrogen; toluene-4-sulfonic acid;
palladium on activated charcoal;
In
acetic acid;
DOI:10.1021/jo00148a012
