(2,3,4-triethylphenyl)-lambda~2~-plumbanyl

Base Information

• Chemical Name: (2,3,4-triethylphenyl)-lambda~2~-plumbanyl
• CAS No.: 878-50-2
• Molecular Formula: C12H17Pb
• Molecular Weight: 371.491
• Mol file: 878-50-2.mol

Synonyms:

Chemical Property of (2,3,4-triethylphenyl)-lambda~2~-plumbanyl

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2,3,4-triethylphenyl)-lambda~2~-plumbanyl

There total 2 articles about (2,3,4-triethylphenyl)-lambda~2~-plumbanyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

triethyllead bromide (41141-89-3) → triethyl-phenyl plumbane (878-50-2)

Guidance literature:

With C₆H₅MgBr; In tetrahydrofuran; byproducts: MgBr2; react. of Pb compd. and Grignard compd.; purity checked by (1)H-NMR;

DOI:10.1016/S0022-328X(00)90533-3

Reference yield:

bromobenzene (108-86-1,52753-63-6) → triethyl-phenyl plumbane (878-50-2)

Guidance literature:

DOI:10.1021/jo50018a009

Reference yield:

hydrogenchloride (7647-01-0,15364-23-5) + chloroform (67-66-3,8013-54-5) + triethyl-phenyl plumbane (878-50-2) → triethyllead chloride (1067-14-7) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1)

Guidance literature:

DOI:10.1021/ja01355a056

upstream raw materials:

bromobenzene

triethyllead bromide

Downstream raw materials:

triethyllead chloride

benzene

Refernces