Technology Process of Plumbane, bromotriethyl-
There total 4 articles about Plumbane, bromotriethyl- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
ethyl acetate;
(Ar); soln. of Br2 in EtOAc was slowly added to stirred soln. of Et4Pb in EtOAc at -80°C until color of mixt. remained yellow; cold mixt. decanted; residue extd. (Et2O, room temp.); evapd.; dried (vac.);
DOI:10.1021/ja021234g
- Guidance literature:
-
With
N-benzyl pyridinium halide;
In
toluene;
at 50 ℃;
Equilibrium constant;
var. solvents and Et3PbCl conc.;
DOI:10.1016/S0022-328X(00)81789-1
