Tridecylcyclohexane

Base Information

• Chemical Name: Tridecylcyclohexane
• CAS No.: 6006-33-3
• Molecular Formula: C19H38
• Molecular Weight: 266.511
• Hs Code.: 2902199090
• European Community (EC) Number: 227-854-9
• DSSTox Substance ID: DTXSID6064080
• Nikkaji Number: J147.991A
• Wikidata: Q81991228
• Mol file: 6006-33-3.mol

Synonyms:Tridecylcyclohexane;N-TRIDECYLCYCLOHEXANE;6006-33-3;1-Cyclohexyltridecane;Cyclohexane, tridecyl-;EINECS 227-854-9;Tridecane, 1-cyclohexyl-;DTXSID6064080;MFCD00045507;BS-23812;CS-0205057;FT-0635938;T0767;D92391

Chemical Property of Tridecylcyclohexane

Chemical Property:

• Vapor Pressure: 0.000121mmHg at 25°C
• Melting Point: 18.51°C
• Refractive Index: 1.4560 to 1.4580
• Boiling Point: 346 °C
• Flash Point: 156.2°C
• PSA: 0.00000
• Density: 0.82
• LogP: 7.26780
• XLogP3: 10
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 12
• Exact Mass: 266.297351212
• Heavy Atom Count: 19
• Complexity: 167

Purity/Quality:

98%,99%, ^*data from raw suppliers

Tridecylcyclohexane >98.0%(GC) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCCCCC1CCCCC1

Technology Process of Tridecylcyclohexane

There total 2 articles about Tridecylcyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

cyclohexylmethyl iodide (5469-33-0) + laurylmagnesium bromide (15890-72-9) → n-tridecylcyclohexane (6006-33-3)

Guidance literature:

With lithium chloride; copper dichloride; In tetrahydrofuran; at 0 ℃; Inert atmosphere;

DOI:10.1039/c7ob02505j

Reference yield: 73.0%

laurylmagnesium bromide (15890-72-9) + cyclohexylmethyl trifluoromethanesulfonate (70869-86-2) → n-tridecylcyclohexane (6006-33-3)

Guidance literature:

With copper(I) bromide dimethylsulfide complex; In tetrahydrofuran; at 0 ℃; Inert atmosphere;

DOI:10.1039/c7ob02505j

upstream raw materials:

cyclohexylmethyl iodide

laurylmagnesium bromide

cyclohexylmethyl trifluoromethanesulfonate

Refernces