AlEt2I

Base Information

• Chemical Name: AlEt2I
• CAS No.: 2040-00-8
• Molecular Formula: C4H10 Al I
• Molecular Weight: 212.009
• Hs Code.: 29310099
• Mol file: 2040-00-8.mol

Synonyms:AlEt2I;SCHEMBL329902;PPQUYYAZSOKTQD-UHFFFAOYSA-M

Chemical Property of AlEt2I

Chemical Property:

• Vapor Pressure: 0.467Pa at 25℃
• Melting Point: -56.9°C
• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 0.00000
• Density: g/cm³
• LogP: 2.83350
• Storage Temp.: water-free area
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 211.96426
• Heavy Atom Count: 6
• Complexity: 11.1

Purity/Quality:

99.9% ^*data from raw suppliers

Safty Information:

• Hazard Codes: C-F
• Statements: 67-65-63-48/20-35-14/15-11
• Safety Statements: 62-46-36/37/39-16

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC[Al+]CC.[I-]

Technology Process of AlEt2I

There total 7 articles about AlEt2I which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

triethylaluminum (97-93-8) + aluminium (7429-90-5) → trimethylaluminum (75-24-1) + diethylaluminum iodide (2040-00-8)

Guidance literature:

With iodine; methyl iodide; In ethanol; Sonication; N2; CH3I, I2 and Al introduced in a condenser with C2H5OH at -20°C, ultrasonic acceleration at room temp. for 2 h, Et3Al (ratio MeI/Et3Al = 1.50) dropped into soln. within 10 min, sonication for 30 min; distilled (vac.);

DOI:10.1016/S0022-328X(00)98951-4

Reference yield:

ethyl iodide (75-03-6) → diethylaluminum iodide (2040-00-8)

Guidance literature:

With aluminium;

DOI:10.3402/tellusb.v52i5.17098

Reference yield:

ethyl iodide (75-03-6) + aluminium (7429-90-5) → diethylaluminum iodide (2040-00-8)

Guidance literature:

In diethyl ether;

upstream raw materials:

ethyl iodide

triethylaluminum

aluminium

Downstream raw materials:

iodine

aluminium

(C₆H₅)2PN(C(CH₃)3)Al(C₂H₅)2

Refernces