4-BROMOBENZALDEHYDE OXIME

Base Information

• Chemical Name: 4-BROMOBENZALDEHYDE OXIME
• CAS No.: 25062-46-8
• Molecular Formula: C7H6 Br N O
• Molecular Weight: 200.035
• Hs Code.: 2928000090
• Mol file: 25062-46-8.mol

Synonyms:Benzaldehyde,4-bromo-, oxime, (Z)-; Benzaldehyde, p-bromo-, oxime, (Z)- (8CI);(Z)-p-Bromobenzaldehyde oxime; anti-4-Bromobenzaldehyde oxime;anti-p-Bromobenzaldoxime

Chemical Property of 4-BROMOBENZALDEHYDE OXIME

Chemical Property:

• Vapor Pressure: 0.00961mmHg at 25°C
• Boiling Point: 253.2°Cat760mmHg
• Flash Point: 107°C
• PSA: 32.59000
• Density: 1.52g/cm³
• LogP: 2.25720

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-BROMOBENZALDEHYDE OXIME

There total 32 articles about 4-BROMOBENZALDEHYDE OXIME which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-bromo-benzaldehyde (1122-91-4) → 4-bromobenzaldehyde oxime (25062-46-8,40979-16-6,34158-73-1)

Guidance literature:

With hydroxylamine hydrochloride;

DOI:10.1039/b305268k

Reference yield: 100.0%

4-bromo-benzaldehyde (1122-91-4) → 4-bromobenzaldehyde Oxime (25062-46-8,34158-73-1,40979-16-6)

Guidance literature:

With pyridine; hydroxylamine hydrochloride; In ethanol;

DOI:10.1021/ol0168768

Reference yield: 96.0%

4-bromo-benzaldehyde (1122-91-4) → (Z)-4-bromobenzaldehyde oxime (25062-46-8)

Guidance literature:

With hydroxylamine hydrochloride; In ethanol; at 20 ℃; for 1h; stereoselective reaction;

DOI:10.1002/jccs.201200011

upstream raw materials:

4-bromo-benzaldehyde

(E)-ethyl 3-(4-bromophenyl)-2-cyanoacrylate

Nitroethane

(S)-2-phenylglycine

Downstream raw materials:

4-bromobenzaldehyde Oxime

Ethyl 4-bromobenzoate

iso-butyl 4-bromobenzoate

(E)-N-(4-bromobenzylidene)-P,P-diphenylphosphinic amide

Refernces

• 1、 -. "Preparation method O - alkyl substituted hydroxylamine salt". Paragraph 0118; 0124-0127. . Retrieved 2021/11/14.
• 2、 Pan, Hongmei,Lu, Tong,Wu, Xuedan,Gu, Chengwen,Tao, Naili,Zhang, Biao,Wang, Ao,Chen, Guangmei,Zhang, Kehua,Cheng, Jie,Jin, Jie. "Design and synthesis of sinomenine isoxazole derivatives via 1,3-dipolar cycloaddition reaction". supporting information. p. 2360 - 2364. Retrieved 2019/11/11.