3-(p-Methoxybenzyl)-4-(p-methoxyphenyl)hexane

Base Information

• Chemical Name: 3-(p-Methoxybenzyl)-4-(p-methoxyphenyl)hexane
• CAS No.: 4468-39-7
• Molecular Formula: C21H28O2
• Molecular Weight: 312.44582
• DSSTox Substance ID: DTXSID80963265
• Nikkaji Number: J73.699F
• Mol file: 4468-39-7.mol

Synonyms:Compound 77/735;CDRI 77/735;BRN 3214677;3-(p-Methoxybenzyl)-4-(p-methoxyphenyl)hexane;4468-39-7;3-06-00-05532 (Beilstein Handbook Reference);HEXANE, 3-(p-METHOXYBENZYL)-4-(p-METHOXYPHENYL)-;Benzene, 1,1'-(1,2-diethyl-1,3-propanediyl)bis(4-methoxy-;1-[2-ethyl-3-(4-methoxyphenyl)pentyl]-4-methoxybenzene;DTXSID80963265;LS-75136;Benzene, 1,1'-(1,2-diethyl-1,3-propanediyl)bis(4-methoxy- (9CI)

Chemical Property of 3-(p-Methoxybenzyl)-4-(p-methoxyphenyl)hexane

Chemical Property:

• Vapor Pressure: 1.02E-06mmHg at 25°C
• Refractive Index: 1.527
• Boiling Point: 415.1 °C at 760 mmHg
• Flash Point: 143 °C
• Density: 0.993 g/cm³
• XLogP3: 6.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 8
• Exact Mass: 312.208930132
• Heavy Atom Count: 23
• Complexity: 301

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCC(CC1=CC=C(C=C1)OC)C(CC)C2=CC=C(C=C2)OC

Technology Process of 3-(p-Methoxybenzyl)-4-(p-methoxyphenyl)hexane

There total 2 articles about 3-(p-Methoxybenzyl)-4-(p-methoxyphenyl)hexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 3-(4-methoxy-benzyl)-4-(4-methoxy-phenyl)-hexane (4468-39-7)

Guidance literature:

With ethanol; copper oxide-chromium oxide; at 230 ℃; under 147102 - 183877 Torr; optically inactive 3-<4-methoxy-phenyl>-4-<4-methoxy-benzyl>-hexane of bp ₂: 180-183 degree; Hydrogenation;

DOI:10.1021/ja01225a019

Reference yield:

ethanol (64-17-5) + 2-ethyl-1,3-bis-(4-methoxy-phenyl)-pentan-1-one (74063-46-0) → 3-(4-methoxy-benzyl)-4-(4-methoxy-phenyl)-hexane (4468-39-7)

Guidance literature:

at 230 ℃; under 147102 - 183877 Torr; optically inactive stereoisomer(ic) of mp: 82 degree; Hydrogenation;

DOI:10.1021/ja01225a019

Reference yield:

3-(4-methoxy-benzyl)-4-(4-methoxy-phenyl)-hexane (4468-39-7) → 3-(4-hydroxy-benzyl)-4-(4-hydroxy-phenyl)-hexane

Guidance literature:

With potassium hydroxide; at 200 ℃; optically inactive 3-<4-hydroxy-phenyl>-4-<4-hydroxy-benzyl>-hexane of mp: 52 degree;

DOI:10.1021/ja01225a019

upstream raw materials:

ethanol

2-ethyl-1,3-bis-(4-methoxy-phenyl)-pentan-1-one