Basic blue 6

Base Information

• Chemical Name: Basic blue 6
• CAS No.: 966-62-1
• Molecular Formula: C₁₈H₁₅N₂O*Cl
• Molecular Weight: 310.783
• European Community (EC) Number: 213-524-1
• NSC Number: 9291
• UNII: CP2ST8ED1O
• DSSTox Substance ID: DTXSID40874040
• Wikidata: Q27275599
• ChEMBL ID: CHEMBL2002549
• Mol file: 966-62-1.mol

Synonyms:9-(dimethylamino)-benzophenoxazinium chloride cpd with zinc chloride;9-methylaminobenzo alpha-phenoxazonium chloride;Meldola blue

Chemical Property of Basic blue 6

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 29.27000
• Density: g/cm³
• LogP: 1.48530
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 0
• Exact Mass: 310.0872908
• Heavy Atom Count: 22
• Complexity: 566

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[N+](=C1C=CC2=NC3=C(C=CC4=CC=CC=C43)OC2=C1)C.[Cl-]

Technology Process of Basic blue 6

There total 3 articles about Basic blue 6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-nitroso-N,N-dimethylaniline hydrochloride (42344-05-8) + β-naphthol (135-19-3) → basic blue 6 (966-62-1,4482-24-0)

Guidance literature:

With acetic acid; at 110 ℃;

Reference yield:

β-naphthol (135-19-3) → basic blue 6 (966-62-1,4482-24-0)

Guidance literature:

With sodium dichromate; zinc(II) chloride; at 70 ℃;

Reference yield:

4-dimethylaminophenylamine dihydrochloride (536-46-9,13806-04-7) + (E)-3-Ureido-but-2-enoic acid ethyl ester (5435-44-9,22243-66-9) + β-naphthol (135-19-3) → basic blue 6 (966-62-1,4482-24-0)

Guidance literature:

at 70 ℃;

upstream raw materials:

4-nitroso-N,N-dimethylaniline hydrochloride

β-naphthol

4-dimethylaminophenylamine dihydrochloride

(E)-3-Ureido-but-2-enoic acid ethyl ester

Downstream raw materials:

(9-dimethylamino-benzo[a]phenoxazin-5-ylidene)-p-tolyl-amine

9-dimethylamino-5-p-toluidino-benzo[a]phenoxazinylium; chloride

[5-(2-carboxy-phenylsulfanyl)-benzo[a]phenoxazin-9-ylidene]-dimethyl-ammonium; chloride

dimethyl-[5-(toluene-4-sulfonyl)-benzo[a]phenoxazin-9-ylidene]-ammonium; chloride