2-Thiophenesulfonyl chloride, 4-(4-methoxybenzoyl)-

Base Information Edit

Chemical Name:2-Thiophenesulfonyl chloride, 4-(4-methoxybenzoyl)-
CAS No.:143509-75-5
Molecular Formula:C12H9ClO4S2
Molecular Weight:316.786
Hs Code.:
Mol file:143509-75-5.mol

Synonyms:

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Chemical Property of 2-Thiophenesulfonyl chloride, 4-(4-methoxybenzoyl)- Edit

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Technology Process of 2-Thiophenesulfonyl chloride, 4-(4-methoxybenzoyl)-

There total 2 articles about 2-Thiophenesulfonyl chloride, 4-(4-methoxybenzoyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 874-90-8
4-methoxybenzonitrile

: 143509-75-5
4-(4-Methoxy-benzoyl)-thiophene-2-sulfonyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi, 3.) aq. HCl

2: H₂SO₄, acetic anhydride / CH₂Cl₂ / 16 h / Ambient temperature

3: thionyl chloride / 1.5 h / Heating

With hydrogenchloride; n-butyllithium; thionyl chloride; sulfuric acid; acetic anhydride; In dichloromethane;
DOI:10.1021/jm00099a010

Reference yield:

: 5064-00-6
(4-methoxyphenyl)(thiophen-3-yl)methanone

: 143509-75-5
4-(4-Methoxy-benzoyl)-thiophene-2-sulfonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: H₂SO₄, acetic anhydride / CH₂Cl₂ / 16 h / Ambient temperature

2: thionyl chloride / 1.5 h / Heating

With thionyl chloride; sulfuric acid; acetic anhydride; In dichloromethane;
DOI:10.1021/jm00099a010