Technology Process of Benzenesulfonic acid, 3-nitro-, [(2S)-2-methyloxiranyl]methyl ester
There total 4 articles about Benzenesulfonic acid, 3-nitro-, [(2S)-2-methyloxiranyl]methyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at -20 - 0 ℃;
for 3h;
- Guidance literature:
-
3-hydroxy-2-methyl-1-propene;
With
titanium(IV)isopropoxide; D-(-)-diisopropyl tartrate;
In
dichloromethane;
at -20 ℃;
for 0.5h;
With
Cumene hydroperoxide;
In
dichloromethane;
at -20 ℃;
3-Nitrochlorobenzene;
With
dmap; triethylamine; phosphorous acid trimethyl ester;
more than 3 stages;
- Guidance literature:
-
3-hydroxy-2-methyl-1-propene;
With
titanium(IV) isopropylate; diethyl (2S,3S)-tartrate;
In
dichloromethane;
at -35 - -20 ℃;
Molecular sieve;
Inert atmosphere;
3-nitrobenzenesulphonyl chloride;
With
dmap; triethylamine; triethyl phosphite;
In
dichloromethane;
at -25 - -10 ℃;
