1,1-Dichloro-2,2-diethoxyethane

Base Information

• Chemical Name: 1,1-Dichloro-2,2-diethoxyethane
• CAS No.: 619-33-0
• Molecular Formula: C6H12Cl2O2
• Molecular Weight: 187.066
• Hs Code.: 29110000
• European Community (EC) Number: 210-591-9
• DSSTox Substance ID: DTXSID7060700
• Nikkaji Number: J134.697K
• Wikidata: Q72465943
• ChEMBL ID: CHEMBL2251329
• Mol file: 619-33-0.mol

Synonyms:619-33-0;1,1-DICHLORO-2,2-DIETHOXYETHANE;2,2-dichloro-1,1-diethoxyethane;Dichloroacetaldehyde diethyl acetal;Dichloroacetal;Ethane, 1,1-dichloro-2,2-diethoxy-;DICHLOROACETALDEHYDEDIETHYLACETAL;EINECS 210-591-9;Dichloracetal;1,1-dichloro-2,2-diethoxy-ethane;MFCD00000849;SCHEMBL7767624;CHEMBL2251329;dichloroacetaldehyde diethylacetal;DTXSID7060700;dichloro-acetaldehyde diethyl-acetal;2,2-Dichloro-1,1-diethoxy ethane;1,1-Dichloro-2,2-diethoxyethane #;2,2-Dichloro-1,1-Diethyoxy Ethane;AKOS015912992;Dichloroacetaldehyde diethyl acetal, 98%;CS-0094729;D0354;FT-0624697;D89635;Dichloroacetaldehyde diethyl acetal, purum, >=97.0% (GC)

Chemical Property of 1,1-Dichloro-2,2-diethoxyethane

Chemical Property:

• Vapor Pressure: 1.05mmHg at 25°C
• Refractive Index: n20/D 1.436(lit.)
• Boiling Point: 183.5 °C at 760 mmHg
• Flash Point: 60 °C
• PSA: 18.46000
• Density: 1.141g/cm³
• LogP: 2.18920
• Storage Temp.: 2-8°C
• XLogP3: 2.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 5
• Exact Mass: 186.0214350
• Heavy Atom Count: 10
• Complexity: 72.1

Purity/Quality:

98%,99%, ^*data from raw suppliers

Dichloroacetaldehyde diethyl acetal ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CCOC(C(Cl)Cl)OCC

Technology Process of 1,1-Dichloro-2,2-diethoxyethane

There total 31 articles about 1,1-Dichloro-2,2-diethoxyethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloroacetaldehyde diethyl acetal (621-62-5) → dichloroacetaldehyde diethyl acetal (619-33-0) + chloroform (67-66-3,8013-54-5) + 1,1,1-trichloro-2,2-diethoxy-ethane (599-97-3) + acetaldehyde (75-07-0,9002-91-9)

Guidance literature:

Reference yield:

1,1,2-trichloro-2-ethoxy-ethane (687-44-5) → dichloroacetaldehyde diethyl acetal (619-33-0)

Guidance literature:

With water;

Reference yield:

ethanol (64-17-5) → dichloroacetaldehyde diethyl acetal (619-33-0)

Guidance literature:

With chlorine;

upstream raw materials:

diethyl acetal

diethyl ether

ethanol

ethyl-(1,2,2,2-tetrachloro-ethyl)-ether

Downstream raw materials:

perthane

2-chloro-1,1-bis-(4-propyl-phenyl)-ethene

1,1-bis-(4-butyl-phenyl)-2-chloro-ethene

1,1-dichloro-2,2-bis-(2,4-dichloro-5-methoxy-phenyl)-ethane

Refernces

• 1、 Griesbaum, Karl,Hayes, Michael P.,Werli, Vera. "Products and reaction pats in the liquid phase oxidation of trans-1,2-dichloroethene with oxygen". . p. 1366 - 1370. Retrieved 2007/10/02.