Technology Process of Acetamide, N-[2-(3-hydroxy-4-methoxyphenyl)ethyl]-
There total 11 articles about Acetamide, N-[2-(3-hydroxy-4-methoxyphenyl)ethyl]- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 94 percent / K2CO3 / ethanol / 5 h / Heating
2: 88 percent / NH4OAc; AcOH / 4 h / Heating
3: 63 percent / LiAlH4 / diethyl ether; tetrahydrofuran / 2 h / Heating
4: 5percent aq. NaOH / CH2Cl2 / 2 h / 20 °C
5: conc. HCl / ethanol / 4 h / Heating
With
hydrogenchloride; lithium aluminium tetrahydride; ammonium acetate; potassium carbonate; acetic acid;
In
tetrahydrofuran; diethyl ether; ethanol; dichloromethane;
4: Schotten-Baumann reaction;
DOI:10.1021/jm020831a
- Guidance literature:
-
With
hydrogenchloride;
In
ethanol;
for 4h;
Heating;
DOI:10.1021/jm020831a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 63 percent / LiAlH4 / diethyl ether; tetrahydrofuran / 2 h / Heating
2: 5percent aq. NaOH / CH2Cl2 / 2 h / 20 °C
3: conc. HCl / ethanol / 4 h / Heating
With
hydrogenchloride; lithium aluminium tetrahydride;
In
tetrahydrofuran; diethyl ether; ethanol; dichloromethane;
2: Schotten-Baumann reaction;
DOI:10.1021/jm020831a