Technology Process of 3,5-Diiodophenol
There total 7 articles about 3,5-Diiodophenol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
1,3,5-Triiodobenzene;
With
n-butyllithium;
In
diethyl ether; hexane;
at -78 - 25 ℃;
With
sodium hydroxide; dihydrogen peroxide;
for 3h;
DOI:10.1021/jo035311h
- Guidance literature:
-
3,5-diiodoaniline;
With
sulfuric acid;
at 0 ℃;
for 0.5h;
Inert atmosphere;
Schlenk technique;
With
sodium nitrite;
at 0 ℃;
for 2h;
Inert atmosphere;
Schlenk technique;
With
sulfuric acid;
for 0.5h;
Inert atmosphere;
Schlenk technique;
DOI:10.1002/chem.201504598
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium dithionit / H2O; 2-methoxy-ethanol / 3 h / Heating
1.2: 94 percent / conc. HCl / H2O; 2-methoxy-ethanol / 1 h / Heating
With
sodium dithionite;
In
2-methoxy-ethanol; water;
DOI:10.1021/ja003990x
