1-Methoxy-3,5-diiodobenzene

Base Information Edit

Chemical Name:1-Methoxy-3,5-diiodobenzene
CAS No.:344324-66-9
Molecular Formula:C7H6I2O
Molecular Weight:359.933
Hs Code.:
Mol file:344324-66-9.mol

Synonyms:1-METHOXY-3,5-DIIODOBENZENE;3,5-DIIODOANISOLE

Suppliers and Price of 1-Methoxy-3,5-diiodobenzene

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-METHOXY-3,5-DIIODOBENZENE 95.00%
5MG
$ 503.91

Total 3 raw suppliers

Chemical Property of 1-Methoxy-3,5-diiodobenzene Edit

Chemical Property:

Boiling Point:345.3 °C at 760 mmHg
Flash Point:162.6 °C
PSA：9.23000
Density:2.284 g/cm³
LogP:2.90440

Purity/Quality:

99% ^*data from raw suppliers

1-METHOXY-3,5-DIIODOBENZENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-Methoxy-3,5-diiodobenzene

There total 5 articles about 1-Methoxy-3,5-diiodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 3,4,5-triiodoanisole

: 344324-66-9
1,3-diiodo-5-methoxybenzene

Guidance literature:: 3,4,5-triiodoanisole; With isopropylmagnesium chloride; In tetrahydrofuran; at -78 ℃; for 2h;

With water; In tetrahydrofuran; at 20 ℃; for 24h; regioselective reaction;
DOI:10.1002/ejoc.201500887

Reference yield:

: 100-09-4
4-methoxybenzoic acid

: 344324-66-9
1,3-diiodo-5-methoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: palladium diacetate; [bis(acetoxy)iodo]benzene; iodine / N,N-dimethyl-formamide / 24 h / 120 °C / Sealed tube; Irradiation

2.1: isopropylmagnesium chloride / tetrahydrofuran / 2 h / -78 °C

2.2: 24 h / 20 °C

With [bis(acetoxy)iodo]benzene; iodine; isopropylmagnesium chloride; palladium diacetate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201500887

Reference yield:

: 5327-44-6
3,5-dinitroanisole

: 344324-66-9
1,3-diiodo-5-methoxybenzene

Guidance literature:: With acetic acid; platinum; Hydrogenation_.Behandlung des Reaktionsprodukts mit Schwefelsaeure, Natriumnitrit und Essigsaeure und anschliessend mit einem Gemisch von Natriumjodid, Jod, Harnstoff, Wasser und Chloroform;